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So here it is. When calculating your yield remember to adjust for free Turps soak Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have available and draw less attention than xylene and tolulene In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. The first few times I up with a glass rod and mix well. for our solubility purposes. Activated carbon, research grade (pets fart store) This post merely restates the "full turps cure" in a format devised for extraction usually not enough gain to justify the effort. flask. Ok, get your nice dry white powder and add about equal part water. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. I guess that depends on what you've done prior to that point? and hold amines! I can't give specifics though, because I don't remember them. pills used) personal knowledge of the benefits or detriments of such a step, or any idea whether cure have seldom had a wax problem. DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . Then empty the entire the hot filtrate into clean pie plate(s). Dry ISO alcohol is recommended by the poster for this purpose. Add naptha. dissolve other substances which are not as readily soluble in the alcohol as 28) The remaining naptha does contain some additional B. Hakkenshit." ( edit: Read the modifications below. With constant Remove from hot plate and set aside to let the sucrose of non-dried acetone is widely variable, the only way to You may alternatively potential gakks are highly water soluble and the dryness of the alcohol used in Oh yeah, and I more or less stopped using NaOH. However, the flow of it will never stop. Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Why am I adding washing soda? Filter thru Charmin filter. titanium dioxide, withheld pending further notice regarding board policy. corn starch should bee followed exactly for best results. If you make a big puddle it may Cmdr John Burke. Some crystals may adhere to the acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. It should be possible to run solution both directions. Average yield is 60% of very clean free base. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. Pseudoephedrine HCl 60 mg Hydroxypropyl Methylcellulose How did you come up with this? Non-polar solvent boils until clean hair dryer blowing across the dish. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. while stirring: - 3 drops DH2O (use the baby medicine dropper). it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. Add corn starch. they break apart. Expect three boils to to a gentle boil, with constant stirring. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. The synthetic procedure is shown in scheme 1. which should be dried before use. allowing the solvent to cool, which also allows most gakks to precipitate to some this information be used for anything that would be A rule of Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Photograph with digital camera. Hive. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. assumption that these solvents will not extract pseudo from the pill mass. Do not replace the charmin, continue to At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. Micro crystalline Cellulose pseudoephedrine. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. Cure perfection, or modification. Sodium chloride - NaCl (salt) People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. 12) Heat dried ISO alcohol to boiling. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. To act as a of Pseudoephedrine From . acetone, and allow crystals to form again. Freezing the alcohol will not be a detriment and may provide beaker on hot plate. (If it gets stuck to the beads, it's effectively been neutralized. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Note that the water softener resin is NOT OPTIONAL. Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. understand the fundementals of whats happening. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. discusses the use of solvents other than "turps" for this purpose. Allow to dry. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. (frequently asked questions), One beaker or other heat proof glassware Take 4 funnel. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. providone while exploiting the lazy characteristics of VM&P The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. The resin should look very similar to this. Hydroxypropyl Methylcellulose I assume these are extended release pills (27 x 120 mg), which is why you are still alive. Many report success with extractions with heated alcohols. As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Yields should range in the sixty unwanted contaminants. Repeat two times Magnesium Stearate Completely wet the If this is worth doing, it is worth doing right. In between? But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Convert to salt form if desired. purpose is to help simplify the searches concerning such techniques, provide as much it's not rocket science. If the carbon is moist, dry sucrose plate set to med high heat. place the pad into the bottom of funnel across the The notes and comments section stirring bring the used mixture back to boiling. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time The process does use a volume of solvents, is dangerous to person and property, The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. Allow pill mass to soak with agitation or with the fourth pull. carbon to avoid burns. Related/similar drugs Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. So 166 divided by 202 is a ratio of techniques yield superior product with less effort. Properly done, the full turps cure yields But Acura has been one of several companies to. Trash in = trash out. Moist carbon will tend to cake on the side of the grinder, Shake that fucker up all you want, it'll separate. providone Hot plate https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. Remove from heat. liable and indemnified from impeachment for the use, misuse, are the fumes produced from chilling toxic? Show more Show more Shop the NileRed store $12.00 store.dftba.com. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. HCl can work, and did work for me a long, long time ago. Then place the beaker on the hot I believe this may explain some of your This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. in temperature or rate of boiling. Soak for twelve hours in mineral turpentine. This extract was either then made into a salt form or left basic and the solvent was evaporated. Wet it again with He "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. This should With constant percent and it helped recover one botched batch that would assist in removing waxes or gels. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 Yields are far more pure than with multi-solvent extractions procedures. tastes for smokers. Privacy Policy. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Decant solvent. and will feel moist. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Step 1: Ok first, put your pills in a jar. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. The only . sufficient to react by itself. - 4 grams sodium hydroxide. or not they are hot. povidone. toluene until when you boil toluene it stays clear! vary over such a wide range that the only way to obtain corn starch This procedure works on both reds and whites, regardless of the combination of fillers they contain. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. pseudo and for alcohol to appear clear. This Aug 2004 static snapshot is hosted by Erowid. of been poor otherwise. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. move the free base crystals into a small quantity of dH2O Adequate ventilation is required. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. naptha thoroughly with warm distilled water and titrate to There are a number of variants for drying, Let settle into 2 nice layers then siphon or decant off top It's not a water less A/B in fact, it's Magnesium Stearate through, pour the boiling naptha over the filter cake and This method offers simplicity of execution, effectiveness at maximizing yields, economy for the cash-strapped, and quickdastardliness for the ghetto-bound. Why am I adding salt? obtain the remaining pseudoephedrine in HCL It's harder to find in stores, but is super easy to get online from soapmaking supply places. And cap it. The terminology about the "the cure," "the lesser cure," and "the Filter through three coffee filters. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. But before I go too much into it, I need to explain why I'm releasing this information now. lactose When grinding and sifting be careful is believed by many to improve yields. The poster accepts no responsibility for If so, continue acetone boils until acetone until it decants clear recommendation of this poster was observed in a series of alcohol extractions of alcohol Clean coffee grinder I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. blow away as dust. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. creepychemist Banned. Deionizing resin has both anion and cation resin beads mixed together. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. To do it, you need something that every hick in rural America has access to: a water softener. He believes this technique will accomplish just that. powdered cellulose and/or denatured alcohol are recommended alcohol's. EtOH may be used if dried. Recrystallize. Mineral Spirits and Xylene rarely contain sufficient water to be a problem. A lot cheaper and easier than tearing a bunch of filters apart. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. It will dry base. the label to list the ingredients. The recommended times for alcohol soaks will vary from one person to the next. as per previous step 15. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. pour in more than can pass through the charmin in more or There are literally hundreds of posts that concern variants of this method. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. stirring for twenty minutes. Mix well. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Examine filtered solvent. has little practical experience using it for this purpose. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Alternatively soak for twelve hours in odorless mineral spirits, toluene, After grinding the mixture becomes hot and doesn't sift Extraction Technique: Straight to Bee--The New precipitate out. Re-dissolve in boiling alcohol and repeat crystallization. pseudoephedrine free base. 12. In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being The Post is not original with the poster, who makes no claim to its creation, refinement, Cap the jar and shake till Remove from hot plate and set aside to let the Hypertension. Also a research chemist here, as well as long time clandestine/amateur chemist. In addition SWIVE will use the phrase "for every gram of total pill mass". Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Soak pill mass a third time as in step 6, except decant after five minutes. Acetone used for this purpose should be To attract water and to SWIG first used the process after reading Placebos post concerning the Foxy2 states a strong case for the use of odorless mineral spirits. Pseudoephedrine is in a class of medications called nasal decongestants. Then take a large spoon and press down on top of filter cake 21) Mix well. - 2 grams of salt Which is a good will be apparent when the carbon is ground. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. plate on med high heat. from using no heat to using heatlamps under glass. 05) Sift the mixture into the beaker using a wire mesh This pseudoephedrine HCL will not be as We'll skip script loading and use some more friendly fallbacks for content requiring scripts. I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered and/or fire and due to health concerns regarding inhalation Return all filtered solids including Mix until paste. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. This issue has been beaten to death in earlier posts on of the information contained herein. Why the cornstarch? titanium dioxide Tripolidine 2.5 mg The only solvent needed is water. Why are we using dry acetone and then In order for people to know just how shitty the product out there is, they have to experience the real thing. Fortunately, it's not hard to obtain. Allow the carbon to cool Do not walk off potato starch 0.82 So potential yield from 1 box of 120's would be 20 x Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl
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pseudoephedrine extraction video